Vacuum Heat Treating Additive Manufactured Components

Additive Manufacturing Heat Treating Services

Solution Annealing, Stress Relieving, Aging, Sintering and More

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Heat Treating Services for Additive Manufacturing

Additive Manufacturing Vacuum Heat Treating
RPM Innovations, Inc. complex titanium hollow ribbon additive manufactured part heat treated at 51 (post heat treating)

 

Why is Heat Treating Important to Metal Additive Manufactured Components?

During 3D printing, differential heating and cooling often introduce internal stresses as each layer fuses to form the part. This process causes contraction and expansion, potentially leading to issues such as cracking, warping, or, in extreme cases, structural failure when the part is subjected to pressure in its final application. Heat treatment can alleviate these stresses by altering the microstructure of the material, resulting in enhanced mechanical properties, including increased strength, hardness, and fatigue resistance.

 

Types of Heat Treatment for Additive Parts

Heat treatment is a crucial step in enhancing the performance and durability of 3D-printed parts. There are four primary methods used, and the choice depends on factors such as geometry, material, and the intended application.

Stress Relieving: Stress relieving minimizes internal stresses by allowing the atoms in the material to rearrange into a more stable configuration. By applying heat, the process smooths out any undesirable interactions between layers. This method is effective for most materials, except for cobalt chrome (CoCr).

Hot Isostatic Pressing (HIP): HIP combines heat and pressure to eliminate internal microporosity, further reducing residual stress. Even parts created via Direct Metal Laser Sintering (DMLS), which achieve nearly 100% density, can benefit from HIP. This process is especially beneficial for materials like Inconel and stainless steel 17-4 PH. 51 collaborates with partners such as and to provide HIP services.

Solution Annealing: Solution annealing enhances the mechanical properties of production-grade parts. The material is heated to a high temperature and rapidly cooled, transforming its microstructure to improve ductility. This method is most commonly used for aluminum parts.

Aging (H900 Aging): Aging strengthens parts by exposing them to elevated temperatures. The heat reinforces imperfections within the metal’s lattice structure, increasing hardness and tensile strength. This method is particularly effective for applications requiring enhanced durability.

 

Since the ultimate goal of Additive Manufacturing is to produce near-net components, thereby eliminating machining waste, vacuum heat treating is well situated to be a lasting partner with printing technologies for many years. Only the vacuum heat treating process can produce the critical temperature uniformity (±2°F) and the vital heating and cooling rates by thermocoupling parts in direct contact with the metal. Additionally, the vacuum heat treating process has the ability to attain vacuum levels of 1 X 10-6 Torr which is necessary to produce the clean oxide-free results. These critical thermal and atmospheric conditions only aid in producing strong, ductile, and crack free metallurgical results that are paramount with the new metallurgy of 3D metal printing.

Clean MIM, PIM and Binder Jet processing as well!

 

Services Offered

 

Materials Processed

  • Titanium
  • Stainless Steels
  • PH Stainless Steels
  • Nickel-based Alloys

 

ISO 9001 and AS9100 RegisteredNadcap Heat Treating Approval LogoMedAccred Heat TreatingITAR Compliant

 

Ask the Expert:

Solar Atmospheres of Western PA’s Director of Sales Outlines a Path for a Successful Heat Treatment on Your Additive Manufactured Parts

Solar Atmospheres of Western PA’s President Discusses Vacuum Heat Treating Additive Manufactured Parts

 

 

FAQs

Although laser powder bed fusion and other additive manufacturing processes typically eliminate cutting oils and coolants found in conventional machining, cleanliness is still essential. Build plates that have been resurfaced by machining can retain oils or debris, and complex geometries often trap loose metal powder. If not removed, these contaminants can discolor parts and contaminate the vacuum furnace. Thorough cleaning and powder removal prior to heat treating help ensure optimal results and protect furnace components.

The required vacuum level depends on the material and applicable specification. Many aerospace additive manufacturing specifications recommend vacuum levels of 1 × 10⁻⁴ Torr or lower, with some requiring 5 × 10⁻⁵ Torr or lower. Equally important is maintaining a clean, leak-tight furnace. Low leak rates are critical when processing titanium, precipitation-hardening stainless steels, zirconium, niobium, and other reactive alloys to achieve bright, contamination-free surfaces.

Proper temperature control begins with calibrated, AMS 2750-compliant furnaces and the use of work thermocouples. However, AM components often remain attached to thick build plates that absorb heat and can delay the printed parts from reaching the required processing temperature. Whenever possible, thermocouples should be placed on representative sections of the printed component—not just the build plate—to verify the actual part temperature and ensure the full thermal cycle is achieved.

Absolutely. Even if the furnace maintains an excellent vacuum throughout the heating cycle, contaminated cooling gases can compromise the final surface quality. The purity, dew point, and oxygen content of nitrogen, argon, helium, or hydrogen process gases should be monitored to ensure they meet specification requirements. High-quality process gases are essential for maintaining clean, bright surfaces and preventing contamination during cooling.

Complex AM geometries often contain varying wall thicknesses, internal passages, and intricate features that can heat and cool at different rates, increasing the potential for distortion. Proper stress-relieving cycles, controlled heating and cooling rates, strategic thermocouple placement, and custom fixturing all help minimize distortion. For particularly challenging designs, collaborating with your heat treater early in the process can identify specialized solutions that improve dimensional stability throughout heat treatment.